E0041
NPDF: A New High-resolution Total Scattering Powder
Diffractometer. Th. Proffen, Los Alamos National Laboratory, LANSCE-12, MS
H805, Los Alamos, NM 87545.
Knowing the atomic structure of materials usually means
determining the crystal structure. However, many modern materials are complex,
and their real structure often is deviated locally from the average crystal
structure in significant ways. It is thus necessary to know the structure on
various length scales, since properties are more directly governed
by local atomic arrangements. But the conventional
crystallographic approach cannot provide a complete picture; it has to be
complemented by local probes such as the Pair Distribution Function (PDF)
method.
The Neutron Powder Diffractometer NPD has recently been
upgraded to become NPDF by adding a large number of detectors to the
backscattering region of the instrument. The upgrade was funded by the National
Science Foundation, Los Alamos National Laboratory, University of Pennsylvania
and other academic institutions. On September 27th, 2002 the
shutter of NPDF opened for the first time. A standard data set suitable for PDF
analysis can be obtained in only two hours. This puts NPDF at the cutting
edge of local structure determination but also serve as development platform for
this new structure analysis tool for disordered and nano-structured
materials. The instrument is available to general users in the 2003 run
cycle.