W0027
Models of Dynamic Disorder in Protein Crystals; Theory and
New Analysis. George N. Phillips, Jr., Jason McCoy, Ryan Bannen, and
Sibsankar Kundu, Dept. of Biochemistry Univ. of Wisconsin-Madison Madison, WI
53706.
Although the end result of most crystallographic analyses is a
static snapshot of a molecule, we know there is both static and dynamic disorder
in the system. The effect of this disorder is not fully accounted for by the
usual Debye-Waller treatment, whether isotropic or anisotropic. Especially for
large molecules, methods that include the effects of coupled motions are needed
to fully account for the observed intensities. Some new methods that extend
beyond TLS treatment will be presented, and a simplified model of protein
motions in crystals that includes the effects of crystal contacts will be
described and compared with experimental results.