W0242

Improvements to the NIST Center for Neutron Research Powder Diffractometer, BT-1. Camille Y. Jones, Judith K. Stalick, Qingzhen Huang, and Brian H. Toby, NIST Center for Neutron Research, National Institute of Standards and Technology, Gaithersburg MD 20854-8562.

A new Fankuchen-cut Ge(533)/(733) monochromator with a 120o take-off angle has recently been installed in BT-1, the high-resolution powder diffractometer at the NIST Center for Neutron Research.. BT-1 has 32 detectors with 5o spacing and offers two in-pile collimation settings (7' and 15') and three monochromator take-off angles (75, 90 and 120 degrees). This allows the instrument configuration to be tailored to suit the experiment at hand. BT-1 routinely operates with a resolution Δd/d of ≈0.15%, a resolution matched by only one other instrument in the U.S. However, this resolution can be improved considerably, to ≈0.08%, when needed. Alternately, throughput can be improved through use of a longer wavelength with slightly relaxed resolution. The new Ge monochromator allows for higher resolution, improved throughput and operation at two wavelengths (1.5 and 1.2 Å). The 1.2 Å mode offers accessible range of reflections to nearly be doubled, with all of the "new data" within the monochromator's optimal resolution condition. Approximately 63 days/year (25%) on BT-1 are available to outside users via a rapid-response proposal system. Access for proprietary measurements is also possible, as well as for collaborative projects. See http//www.ncnr.nist.gov/xtal for more details on access.